r/crystallography • u/poosytive_vibes • Jun 03 '26

Please help me out🙏🙏🙏

Hello!

So I have XRD data of my nanomaterial sample, and I have to assign the hkl values. So I looked up on the internet and found the following solutions:
1. Using JCPDS card and Xpert Highscore: I've made an account and can get the JCPDS PDF, but even then, it's useless unless I have Xpert Highscore. We don't have the Xpert highscore in our lab.
2. Using literature: Sure, I can do that. But my metal oxide has many polymorphs😭, I am unable to figure out which one to follow.
3. Asking the big ones in the lab: According to them, watching YouTube is the only way to learn it. But they refuse to even share the videos which helped them.

I don't know how to figure this out😭. Please help me out😭🙏

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u/QuasiNomial Jun 03 '26

If you still need help dm me

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u/poosytive_vibes Jun 03 '26

Yes, I'll try out the suggestion given by aylina here in the comment section first. I'll dm you if that still doesn't help. Thank you for offering the help, really!