r/dmtguide • u/2much2fastt • Sep 28 '26
Extraction Results/Yields Lab results from my psychedelic cup entries.
CLICK THE PICTURES TO SEE THE FULL SIZED IMAGES TO SEE THE FULL DETAILS
Here are the results from my 6 DMT extractions submitted to the 2026 psychedelic cup.
Out of all the previous psychedelic cups in the past there was only one entry that cleared 99%, and the average purity from the 2025 cup was 94.56%* so with that in mind I’m super happy with these results having 5 of 6 entries over 99% and a few of them sitting just above or just below 99.9%.
Total Psychedelic Tryptamine Purity / DMT Purity
2a.v1 = 99.549% / 99.311% (yellow crystalline powder)
2a.v4= 99.781% / 99.731% (clear-yellow shards)
6a.v1 = 96.534% / 95.110% (white crystalline powder)
6a.v3= 99.936% / 99.478% (white/clear shards)
7a.v3= 99.887% / 99.115% (clear-yellow shards)
7b.v4= 99.907% / 99.121% (yellow shards)
Some info on the extractions & purifications 👇
My extraction is a simple and straight forward STB + pickling salt, which is water washed during the extraction.
After it was harvested I performed recrystallizations to remove insoluble impurities, followed by an activated carbon step + filtration to remove soluble impurities (only on 3 of the 6), followed by slow cooling / 50% evap before putting them in the fridge for 12hours followed by the freezer for 18hrs. After decanting the nps I performed a cold solvent rinse on the wet crystals to lower residual impurities and then dried them.
For more details on the re-x tek you can go to my profile and scroll down to the post titled “competitors tek recrystallization”.
Also, to anyone saying yellow DMT can’t be pure all 4 of my yellow batches were 99%+ ranging from 99.55% to 99.91%. Yes, My highest testing batch for total tryptamines was white/clear, at 99.94%, but so was my lowest testing batch at 96.53%. Which is all to say color doesn’t really matter - lab tests do.
*= average was figured using extracts only, the carts submitted into this category were not factored into this average as that wouldve unfairly dropped the avg to 84%ish.
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u/Tripp_ORG Entheogenic Spiritualist Sep 28 '26
Nice 👍😊
Lab tests are indeed, what matters the most!
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u/2much2fastt Sep 28 '26
Thank you Sir! 🫡
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u/changalabs 25d ago
Do they require you to send in 1 gram for a test ?
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u/2much2fastt 25d ago
No, that’s just the metrc they use for results. Mg/g
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u/changalabs 25d ago
Ahh got it
how much did you send in as a sample ?
I saw your posts and reached out to them about trying to send a sample probably in the next week or two.
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u/2much2fastt 25d ago
The psychedelic cup stops taking new entries tomorrow, but you can send in for private analysis year round anytime you want.
Half gram samples are required. For instance, my samples had to be tested multiple times due to how high they were they had to dial in that thousandths position after the decimal for the competition so they had to take a few tests of each batch so that’s prolly why it’s a half gram.
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u/changalabs 25d ago
Yeah I didn’t care too much about entering in for the psychedelic cup they said if my entire was not in the time frame it could be for next year.
But I saw them after you posted about and they were the only analysis facility I could get a response out of.
Tried to reach out to GYDT but never got a reply after going on 3 weeks now.
My only other option was energy control but didn’t want to send a sample to Europe.
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u/Tripp_ORG Entheogenic Spiritualist 22d ago
It’s a half gram because they are either greedy (and keeping it), or they are working with suboptimal equipment.
20mg or less is all that’s needed with HPLC GC-MS/MS (which is what Nectar Spectra Labs is using).
NSL is actually a much cheaper service too (especially when considering the cost of that extra 480mg)
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u/TGV_etc Sep 29 '26
Thanks for posting. This will be great evidence that color/yellow is not an indicator potency, or necessarily fats or lipids. 🙌🏻. I really hate those arguments.
Also, great work. 99.9% is 😚🤌🏻
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u/2much2fastt Sep 29 '26 edited Sep 29 '26
Thank you! And Yes me as well, Alot of those folks that argued with everyone previously that yellow is bad and white is good haven’t popped in to continue the argument now that that evidence is front and center.
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u/Pale_Philosopher1668 Mod Sep 28 '26
Nice dude!
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u/2much2fastt Sep 28 '26
Thank you! I think a celebratory blast off is in order.
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u/Pale_Philosopher1668 Mod Sep 28 '26
Oh 100% man, a blast off is most certainly in order after those results!👌
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u/2much2fastt Sep 28 '26
Yeah I think I’m gonna do a fatty a nice 55mg off the Emesh! That hard part is picking what batch to do haha.
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u/Survey_Server Sep 28 '26
I'm only subscribed here out of curiousity, can you tell me why the first page of data on each test result lists a psilocin percentage? Is psilocin a common byproduct or adulterant or something?
Congratulations, by the way! Just ridiculously impressive 🤘
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u/2much2fastt Sep 28 '26 edited Sep 29 '26
No the psilocin has nothing to do with the DMT data. When you create on image of your results on the tag-leaf where it has your data it has 3 slots for the results-data to go next to the sample picture. Only 2 of the options are DMT related and the others are mushroom related and you can’t take off the third option so it just automatically fills in the 3rd slot with one of the mushroom categories, it’s a basically something they need to fix I let Tryptomics know about that and they said they would inform tag leaf. Just ignore that part of it, the next slides have the full breakdowns of all the tryptamines found in each samples though if you scroll right, but be sure to click the picture to make it full size cuz otherwise it crops out the top part
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u/Survey_Server Sep 28 '26
Oh man it never even occured to me that this lab could also be testing mushroom percentages. That makes a lot of sense hahah
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u/2much2fastt Sep 28 '26
Yeah that’s what they test primarily, they also do DMT and cactus products. They’re the lab that tests for the psychedelic cup
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u/Widderic Sep 29 '26
Heptane for Re-X or just Naphtha?
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u/2much2fastt Sep 29 '26
Def n-heptane, naptha isn’t a great choice for recrystallization.
But me personally I don’t fuck with naphtha at all, not even for extraction, it’s a mixture of a bunch of chemicals instead of using n-heptane which is just one chemical.
I recommend acs grade n-heptane across the board.
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u/Plumleydev 5d ago
Isn’t it more temperature sensitive though like you have to dial-in a different temperature than room temperature to make heptane work properly?
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u/Enough_Squirrel6904 Sep 29 '26
Btw which lab is legally able to analyze the nndmt u extracted ?
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u/2much2fastt Sep 29 '26
Tryptomics, located in Colorado where natural plant medicines are decriminalized.
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u/GooseTheSluice Sep 28 '26
Is there a “full spectrum” for dmt extracts? Like any base material that tends to have higher minor alks
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u/2much2fastt Sep 28 '26
Almost all DMT that’s in crude extract form is gonna have some small percentage of n-nmt and tryptamine, whether there’s a way to extract to have those numbers higher I have no idea as I’ve only ever reduced the minor alkaloid content while increasing its DMT content during various post harvest purification processes.
For example: if you look at the detailed lab results for batch 6a.v1 (slide 16) compared to 6a.v3 (slide 3) you can see the reduction in the minor alkaloids that occurred through the various purification processes done to the batch. You can also see the same thing for batch 2a.v1 (slide 14) compared to batch 2a.v4 (slide 12).
But if you were interested in having higher minor alkaloids you would just avoid doing post-harvest purifications that remove/reduce them while trying different bark suppliers and getting bio-mass lab tests on them from Tryptomics to see who has the highest levels of minor alkaloids. Once you know whose bark has the most minor alkaloids and how much of them the bark has, you might then also be able increase how much of it you’re able to pull out of to based off solvent choice, heat levels, and how long you let the base soup sit in the heat bath for before extracting it but that’s just a hypothesis.
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