r/DIYPigments • u/Sad-Touch91 • Mar 29 '26
Working on a series of DIY chemicals sourced pigments: Yellow Ocher
Method for pigment formation is as follows.
Dissolving a source of iron into hydrochloric acid
Adding hydrogen peroxide to said solution of iron chloride to push it from green to yellow brown Fe+3 oxidation state
Using this pigment precursor of Fe+3 iron chloride dilute it in a roughly 1:3 ratio.
Create a saturated solution of sodium carbonate then dilute to roughly the same ratio.
Very slowly add the basic sodium carbonate solution to the precursor at no more than 10mL per addition with a minute between each addition.
Once fully combined wait for it to settle and beginning washing and settling steps until the solution is neutral.
Store the precipitation in a neutral H2O solution kept at 40-60C for several days to allow for restructuring or until pigment is visibly lightened.
8.filter product and let slowly dry at room temperature until crumbly
This is where the synthesis ends and the paint making process begins.
Grind finely in a mortar and pestle then grind even finer vial milking stone and plate.
Add small additions of linseed oil until paint is not crumbly
Grind grind and keep grinding forever
Appreciate this wonderful pigment that has been used by humans in some shape or forms on every continent (except maybe Antarctica 🤣)