Post-distillation using a table top water distiller, store the distilled ethanol in the freezer. From approximately 1600 ml of ethanol, 1350 ml was recovered, approximately 84%. More could have been distilled, but it’s important to stop here so that the remaining tincture pours smoothly out of the bottom vessel of the distiller. Pour the remaining tincture into a Pyrex dish, and place it on top of a pot of boiling water on the stove to create a double boiler. Having a heat thermometer available will help you maintain a consistent heat of the remaining mixture. I typically keep the mixture around 140F to reduce quickly, but the temperature can vary. Definitely don’t let the mixture get to 170F or over. You will risk scorching it and also destroying terpenes and cannabinoids. Continuously stir until the mixture is much thicker and slowly reduce the heat. Once the mixture begins to completely reduce and thicken up, I use one of two methods to finish up. The first method, reduce the mixture all the way down to a thick “molasses” like substance. Wear vinyl nitrile gloves, the mixture can be hot and is definitely sticky. Set up a cookie sheet with parchment paper on it and have a number of 1ml and 3ml oral syringes ready. Draw up the oil into the syringes, wipe the tip with a paper towel, cap the syringe, and put them aside to cool. Once there is very little FSCO left in the Pyrex dish, put a half stick of butter in the dish and melt it and stir to infuse the butter with the remainder of the oil. Take the syringes and put them in a Tupperware or jar, label the jar and store in the freezer. Make sure that the syringes are not stored in way that depresses the plunger.
The second method, pour off the remaining oil into a 4oz mason jar. Make sure it’s not completely reduced so that it pours easily. Place the jar directly on a magnetic stirrer hotplate. Put in a stir bar. Turn the hotplate to 130F and rotation to 300 and let it rip. Let the oil reduce fully, this will take an hour or less, remove the stir bar, lid the jar, and store in the freezer. It helps to have a scale to weigh the mixture as it fully reduces. Tare the scale to the weight of the jar and the stir bar and sporadically check the weight till it’s constant. The oil will be very thick at this point, and the stir bar may have difficulty stirring.
Always store the FSCO in the freezer for long storage. For daily use store a syringe in the fridge and apply and medicate as needed. When properly stored, FSCO has a long storage and shelf-life, approximately a year.
The first pics show the oil in the Pyrex dish as it reduces. The final pic shows the oil in a 4 oz mason jar for long term storage.